HCID 20504105, compound → HCID 20484937, compound

HRID 1702123Notes

Reaction equation

HRID 1702123 reaction equation
[Br:1][C:2]1[CH:7]=[CH:6][C:5]([N:8]2[C:16](=[O:17])[C:15]3(O)[CH:10]([CH2:11][CH2:12][CH2:13][CH2:14]3)[C:9]2=[S:19])=[C:4]([F:20])[CH:3]=1.BrC1C=CC(N2C(Cl)C3CCCCC=3C2=O)=C(F)C=1>>[Br:1][C:2]1[CH:7]=[CH:6][C:5]([N:8]2[C:9](=[S:19])[C:10]3[CH2:11][CH2:12][CH2:13][CH2:14][C:15]=3[C:16]2=[O:17])=[C:4]([F:20])[CH:3]=1

Participants

3

Reactant 2

HCID 20504105HCID 20504105, compoundHCID 20504108HCID 20504108, compound

Product 1

HCID 20484937HCID 20484937, compound

Procedure

By the same procedure as described in Example 4, there was obtained the subject compound in red-purple crystals of 97° to 98° C. in melting point from 2-(4-bromo-2-fluorophenyl)-3a-hydroxy-1-thioxo-octahydroisoindol-3-one or 2-(4-bromo-2-fluorophenyl)-3-chloro-2,3,4,5,6,7-hexahydro-1H-isoindol-1-one.

Workup

  1. customthere was obtained the subject compound in red-purple crystals of 97° to 98° C.

Sources & evidence

ORD record
ord-29f32b133e3a444d8c465875b61da8cf
Source dataset
uspto-grants-1983_04
Patent number
US04380466

Reaction notes

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