HuagongsheHuagongshe Chemistry Print Report · For research reference only
Chloroform → 2,6-Diethylphenylisonitrile
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Chloroform | HCID 6212 | — |
| Reactant | 2,6-Diethylaniline | HCID 11369 | — |
| Reactant | Sodium Hydroxide | HCID 14798 | — |
| Catalyst | Benzyl triethylammonium chloride | HCID 66133 | — |
| Solvent | Dichloromethane | HCID 6344 | — |
| Product | 2,6-Diethylphenylisonitrile | HCID 151057 | — |
Reaction Steps
The procedure of Example 1 was again followed, using 75 g (0.5 mole) of 2,6-diethylaniline, 60 ml of chloroform, 100 ml of methylene chloride, 200 ml of 50% aqueous sodium hydroxide, and 700 mg of benzyltriethylammonium chloride. The product was an oil weighing 36 g, with structure confirmed by mass spectroscopy.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04380468 |
| Source dataset | uspto-grants-1983_04 |
| ORD ID | ord-d7d8fef0fb0047a0af787c1fa2ec8325 |
| Source note | uspto-grants-1983_04 |