Cyclohexylamine → HCID 86738842, compound

HRID 1702131Notes

Reaction equation

[CH:1]1([NH2:7])[CH2:6][CH2:5][CH2:4][CH2:3][CH2:2]1.Cl[P:9]1[C:14]2[CH:15]=[CH:16][CH:17]=[CH:18][C:13]=2[C:12]2[CH:19]=[CH:20][CH:21]=[CH:22][C:11]=2[O:10]1>>[CH:19]1[C:12]2[C:13]3[CH:18]=[CH:17][CH:16]=[CH:15][C:14]=3[P:9]([N:7]([P:9]3[C:14]4[CH:15]=[CH:16][CH:17]=[CH:18][C:13]=4[C:12]4[CH:19]=[CH:20][CH:21]=[CH:22][C:11]=4[O:10]3)[CH:1]3[CH2:6][CH2:5][CH2:4][CH2:3][CH2:2]3)[O:10][C:11]=2[CH:22]=[CH:21][CH:20]=1

Participants

Reactant 2

HCID 7965Cyclohexylamine

HCID 898166H-Dibenz[c,e][1,2]oxaphosphorin, 6-chloro-

Product 1

HCID 86738842HCID 86738842, compound

Procedure

By using the molar equivalent of cyclohexylamine and two molar equivalents of 6-chloro-dibenz[c,e][1,2]oxaphosphorine, under otherwise the same conditions as those described in Example 1, there is obtained N,N-bis-(dibenz[c,e][1,2]oxaphosphorin-6-yl)-N-cyclohexylamine having a melting point of 191° C. (Compound III).

Sources & evidence

ORD record: ord-c6b39134e02a45c189819e4d38f62936
Source dataset: uspto-grants-1983_04
DOI: 10.6084/m9.figshare.5104873.v1
Patent number: US04380515

Reaction notes

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