HuagongsheHuagongshe Chemistry Print Report · For research reference only
Methyl Acrylate → HCID 12903398, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Methyl Acrylate | HCID 7294 | — |
| Reactant | 3,5-Dimethoxyaniline | HCID 66301 | — |
| Solvent | Acetic Acid | HCID 176 | — |
| Product | HCID 12903398 | HCID 12903398 | 73.9% |
Reaction Steps
A mixture of 3,5-dimethoxyaniline (114.9 g., 0.75 mole), methyl acrylate (69.73 g., 0.81 mole) and glacial acetic acid (2 ml.) is refluxed for 20 hours. Reflux is disconnected and the reaction mixture is concentrated and then distilled in vacuo, to yield 106.8 g. (73.9%) of the title product, b.p. 174°-179° C. (0.7 mm.).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04380542 |
| Source dataset | uspto-grants-1983_04 |
| ORD ID | ord-929ec9a0c02147b8aac4e888f5f71a20 |
| Source note | uspto-grants-1983_04 |