反应详情

In an autoclave, 28.6 g. of 3,5-diaminochlorobenzene, 85 g. of 20% ammonia water and 1.0 g. of cuprous chloride were charged to react them at 175° to 180° C. for 8 hours to obtain 1,3,5-triaminobenzene. Ammonia was discharged and the product was recrystallized to obtain 20 g. of 1,3,5-triaminobenzene.

1. customto react them at 175° to 180° C. for 8 hours