Ammonia → HCID 178483199, compound

HRID 1702289Notes

Reaction equation

HRID 1702289 reaction equation
CO[C:3]1[C:7](OC)=[N:6][S:5](=[O:11])(=[O:10])[N:4]=1.[CH3:12][N:13]([CH2:15][C:16]1[CH:17]=[C:18]([CH2:22][S:23][CH2:24][CH2:25][NH2:26])[CH:19]=[CH:20][CH:21]=1)[CH3:14].[NH3:27]>>[CH3:14][N:13]([CH2:15][C:16]1[CH:17]=[C:18]([CH2:22][S:23][CH2:24][CH2:25][NH:26][C:3]2[C:7]([NH2:27])=[N:6][S:5](=[O:11])(=[O:10])[N:4]=2)[CH:19]=[CH:20][CH:21]=1)[CH3:12]

Participants

4

Reactant 3

HCID 222AmmoniaHCID 122305383,4-Dimethoxy-1,2,5-thiadiazole 1,1-dioxideHCID 129520192-[[3-(N,N-Dimethylaminomethyl)phenyl]methylthio]ethanamine

Product 1

HCID 178483199HCID 178483199, compound

Procedure

When a methanolic suspension of 3,4-dimethoxy-1,2,5-thiadiazole 1,1-dioxide is successively treated with an equimolar amount of 2-[(3-{dimethylaminomethyl}phenyl)methylthio]ethylamine [prepared according to the procedure described in Belgian Pat. No. 867,106] and excess ammonia by the general procedure described in Example 35, the title compound is thereby produced.

Workup

  1. customprepared

Sources & evidence

ORD record
ord-427bf59438e34af48fad1f40085c9e53
Source dataset
uspto-grants-1983_04
Patent number
US04380638

Reaction notes

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