HuagongsheHuagongshe Chemistry Print Report · For research reference only
Methylamine → Orf 17583
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Methylamine | HCID 6329 | — |
| Reactant | 5-(((2-Aminoethyl)thio)methyl)-N,N-dimethyl-2-furanmethanamine | HCID 162203 | — |
| Reactant | 3,4-Dimethoxy-1,2,5-thiadiazole 1-oxide | HCID 12913947 | — |
| Reactant | 3-Methoxy-4-methylamino-1,2,5-thiadiazole 1-oxide | HCID 20030784 | — |
| Product | Orf 17583 | HCID 5486884 | — |
Reaction Steps
Reaction of a methanolic solution of 3,4-dimethoxy-1,2,5-thiadiazole 1-oxide [prepared in Example 4, Step A] with one equivalent of methylamine and treatment of the resultant 3-methoxy-4-methylamino-1,2,5-thiadiazole 1-oxide with one equivalent of 2-[(5-dimethylaminomethyl-2-furyl)methylthio]ethylamine yields the title compound, which is identical to the product prepared in Example 18.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04380639 |
| Source dataset | uspto-grants-1983_04 |
| ORD ID | ord-bd870e9d9a1d40e0a1c302a8fd14e334 |
| Source note | uspto-grants-1983_04 |