HuagongsheHuagongshe Chemistry Print Report · For research reference only
Ammonia → 3-Amino-4-{2-[(6-dimethylaminomethyl-2-pyridyl)methylthio]ethylamino}-1,2,5-thiadiazole 1-oxide
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Ammonia | HCID 222 | — |
| Reactant | 3,4-Dimethoxy-1,2,5-thiadiazole 1-oxide | HCID 12913947 | — |
| Reactant | 2-[(6-Dimethylaminomethyl-2-pyridyl)methylthio]ethylamine | HCID 21292015 | — |
| Product | 3-Amino-4-{2-[(6-dimethylaminomethyl-2-pyridyl)methylthio]ethylamino}-1,2,5-thiadiazole 1-oxide | HCID 15964149 | — |
Reaction Steps
When a methanolic solution of 3,4-dimethoxy-1,2,5-thiadiazole 1-oxide is successively treated with an equimolar amount of 2-[(6-dimethylaminomethyl-2-pyridyl)methylthio]ethyalmine [prepared in Step C] and excess ammonia, the title compound is thereby produced.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04380639 |
| Source dataset | uspto-grants-1983_04 |
| ORD ID | ord-a1ec90edd3cf40c4b4424c1505e277a9 |
| Source note | uspto-grants-1983_04 |