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HRID1702437

反应详情

EQUATION

反应方程式

HRID 1702437 的结构方程式

REACTANTS

反应物

3
结构：O=S(Cl)Cl
HCID24386

Thionyl chloride

Cl2OS

结构：Nc1cccnc1Cl
HCID80528

2-Chloro-3-pyridylamine

C5H5ClN2

结构：Cn1ncc([N+](=O)[O-])c1C(=O)O
HCID592623

1-Methyl-4-nitro-1H-pyrazole-5-carboxylic acid

C5H5N3O4

PRODUCTS

生成物

1
结构：Cn1ncc([N+](=O)[O-])c1C(=O)Nc1cccnc1Cl
HCID20503812

未命名化合物

AUXILIARIES

试剂、催化剂与溶剂

1
结构：CN(C)P(=O)(N(C)C)N(C)C
溶剂HCID12679

Hexamethylphosphoramide

C6H18N3OP

PROCEDURE

实验过程

Prepared analogously to Example A(a) from 1-methyl-4-nitro-1H-pyrazole-5-carboxylic acid, thionyl chloride, and 2-chloro-3-aminopyridine in hexamethylphosphoric acid triamide.