HuagongsheHuagongshe Chemistry Print Report · For research reference only
Thionyl Chloride → 2-[4-(2-Methylpropyl)phenyl]butanoyl chloride
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Thionyl Chloride | HCID 24386 | — |
| Reactant | Butibufen | HCID 41643 | — |
| Product | 2-[4-(2-Methylpropyl)phenyl]butanoyl chloride | HCID 6454130 | 98.1% |
Reaction Steps
110 g of 2-(4-isobutylphenyl)butyric acid and 89 g of thionyl chloride are heated on a water bath until the gas evolution ceases. An excess of thionyl chloride is removed by distillation, A residue of 117 g of 2-(4-isobutylphenyl)butyric chloride is obtained.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04381313 |
| Source dataset | uspto-grants-1983_04 |
| ORD ID | ord-5c56c0aa59364e53800091701c24cecd |
| Source note | uspto-grants-1983_04 |