HuagongsheHuagongshe Chemistry Print Report · For research reference only
Trimethyl orthoformate → 8-Oxo-2-methoxy-3-oxa-1-azabicyclo[4.2.0]octane
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Trimethyl orthoformate | HCID 9005 | — |
| Reactant | HCID 12769226 | HCID 12769226 | — |
| Reactant | HCID 12769229 | HCID 12769229 | — |
| Product | 8-Oxo-2-methoxy-3-oxa-1-azabicyclo[4.2.0]octane | HCID 19993997 | — |
Reaction Steps
Following the procedure described for the preparation of 8-oxo-2,2-dimethyl-3-oxa-1-azabicyclo[4.2.0]octane from 4-(2'-hydroxyethyl)-2-azetidinone and using trimethyl orthoformate instead of 2,2-dimethoxypropane one obtains 8-oxo-2-methoxy-3-oxa-1-azabicyclo[4.2.0]octane.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04348320 |
| Source dataset | uspto-grants-1982_09 |
| ORD ID | ord-fbef1836743b4249aca91b33e213ff6e |
| Source note | uspto-grants-1982_09 |