HuagongsheHuagongshe Chemistry Print Report · For research reference only
1-Bromohexadecane → HCID 13019275, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 1-Bromohexadecane | HCID 8213 | — |
| Reactant | Potassium Carbonate | HCID 11430 | — |
| Reactant | 4-Aminobenzonitrile | HCID 13396 | — |
| Solvent | Water | HCID 962 | — |
| Solvent | Hexamethylphosphoramide | HCID 12679 | — |
| Product | HCID 13019275 | HCID 13019275 | — |
Reaction Steps
A sample of p-aminobenzonitrile is treated at 135° for 15 hours with equimolar quantities of 1-bromohexadecane and anhydrous potassium carbonate in hexamethylphosphoramide. Upon cooling the mixture is diluted with water and extracted with ether. Evaporation of the ether extracts and recrystallization of the residue yields p-(hexadecylamino)benzonitrile.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04348399 |
| Source dataset | uspto-grants-1982_09 |
| ORD ID | ord-a1c1ced5b98845e3b768a7eeab4add56 |
| Source note | uspto-grants-1982_09 |