HCID 20525757, compound → HCID 20525933, compound

HRID 1702680Notes

Reaction equation

HRID 1702680 reaction equation
[CH2:1]([NH:17][C:18]1[CH:30]=[CH:29][C:21]([CH2:22][CH2:23][C:24](OCC)=[O:25])=[CH:20][CH:19]=1)[CH2:2][CH2:3][CH2:4][CH2:5][CH2:6][CH2:7][CH2:8][CH2:9][CH2:10][CH2:11][CH2:12][CH2:13][CH2:14][CH2:15][CH3:16].[H-].[Al+3].[Li+].[H-].[H-].[H-]>>[CH2:1]([NH:17][C:18]1[CH:30]=[CH:29][C:21]([CH2:22][CH2:23][CH2:24][OH:25])=[CH:20][CH:19]=1)[CH2:2][CH2:3][CH2:4][CH2:5][CH2:6][CH2:7][CH2:8][CH2:9][CH2:10][CH2:11][CH2:12][CH2:13][CH2:14][CH2:15][CH3:16]

Participants

3

Reactant 2

HCID 20525757HCID 20525757, compoundHCID 21226445Aluminium lithium hydride

Product 1

HCID 20525933HCID 20525933, compound

Procedure

By a method analogous to that described in Example 16, ethyl 4-hexadecylaminohydrocinnamate is reduced with lithium aluminum hydride to provide the title compound.

Sources & evidence

ORD record
ord-7ed21ca3d1d34672b567646bd40f2c2f
Source dataset
uspto-grants-1982_09
Patent number
US04348399

Reaction notes

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