HuagongsheHuagongshe Chemistry Print Report · For research reference only
Phenol → HCID 20525897, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Phenol | HCID 996 | — |
| Reactant | Sodium hydride | HCID 24758 | — |
| Reactant | 1,1'-Carbonyldiimidazole | HCID 68263 | — |
| Reactant | HCID 20525746 | HCID 20525746 | — |
| Solvent | Tetrahydrofuran | HCID 8028 | — |
| Product | HCID 20525897 | HCID 20525897 | — |
Reaction Steps
A solution of 0.05 mole of 4-(hexadecylamino)hydrocinnamic acid and 0.05 mole of 1,1'-carbonyldiimidazole in 50 ml. of tetrahydrofuran is treated with 0.052 mole of phenol and a trace of sodium hydride. The reaction is heated to reflux for 3 hours, then cooled, filtered and evaporated in vacuo providing phenyl 4-(hexadecylamino)hydrocinnamate.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04348399 |
| Source dataset | uspto-grants-1982_09 |
| ORD ID | ord-860c6ac6c7244512950ac7540aa55d53 |
| Source note | uspto-grants-1982_09 |