HuagongsheHuagongshe Chemistry Print Report · For research reference only
Chloroform → HCID 70507422, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Chloroform | HCID 6212 | — |
| Reactant | Ethyl Acetate | HCID 8857 | — |
| Reactant | HCID 131712810 | HCID 131712810 | — |
| Catalyst | Zinc | HCID 23994 | — |
| Solvent | Acetic acid tetrahydrofuran | HCID 23444217 | — |
| Product | HCID 70507422 | HCID 70507422 | — |
Reaction Steps
By the method of Example 2, pivaloyloxymethyl 1-hydroxy-2-methylcarbapen-2-em-3-carboxylate is reduced with specially activated zinc powder in acetic acid-tetrahydrofuran, the reaction monitored by tlc (4:1 chloroform:ethyl acetate) and the product isolated to yield pivaloyloxymethyl 1-hydroxy-2-methylcarbapenam-3-carboxylate.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04348264 |
| Source dataset | uspto-grants-1982_09 |
| ORD ID | ord-4561dc56cc7945f497a026bee5fc1197 |
| Source note | uspto-grants-1982_09 |