Participants
| Role | Name | HCID | Charge |
|---|
| Reactant | Pyridine | HCID 1049 | — |
| Reactant | 1-Adamantanecarboxylic acid | HCID 13235 | — |
| Reactant | P,P-Diphenylphosphinic azide | HCID 199401 | — |
| Product | 1-Isocyanatoadamantane | HCID 2059995 | — |
Reaction Steps
Diphenylphosphoryl azide (9.08 g.) was added dropwise to a solution of 1-admantanecarboxylic acid (5.4 g.) in dry pyridine (25 ml.) and stirred at 70° C. for one hour to give 1-adamantyl isocyanate [I.R.: 2250 cm-1 ].
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| Patent number | US04349552 |
|---|
| Source dataset | uspto-grants-1982_09 |
|---|
| ORD ID | ord-5b7763b6ed6a445f8c3666d913eab2d6 |
|---|
| Source note | uspto-grants-1982_09 |
|---|
