Sodium Hydroxide → HCID 12961715, compound

HRID 1702900Notes

Reaction equation

HRID 1702900 reaction equation
C[O:2][C:3](=[O:29])[CH2:4][CH2:5][CH2:6][CH2:7][CH2:8][CH2:9][CH2:10][N:11]1[CH:15]=[C:14]([C:16]2[CH:21]=[CH:20][CH:19]=[CH:18][CH:17]=2)[N:13]([C:22]2[CH:27]=[CH:26][CH:25]=[CH:24][CH:23]=2)[C:12]1=[O:28].[OH-].[Na+]>C(O)C>[C:22]1([N:13]2[C:14]([C:16]3[CH:21]=[CH:20][CH:19]=[CH:18][CH:17]=3)=[CH:15][N:11]([CH2:10][CH2:9][CH2:8][CH2:7][CH2:6][CH2:5][CH2:4][C:3]([OH:29])=[O:2])[C:12]2=[O:28])[CH:23]=[CH:24][CH:25]=[CH:26][CH:27]=1

Participants

4

Reactant 2

HCID 14798Sodium HydroxideHCID 12961709HCID 12961709, compound

Product 1

HCID 12961715HCID 12961715, compound

Reagents, catalysts & solvents 1

HCID 702EthanolSolvent

Procedure

The product is produced as described in example 18 from 8.2 g of 8-(3.4-diphenyl-2-oxo-4-imidazolin-1-yl) caprylic acid methyl ester and 0.84 g of NaOH in 20 cc. of ethanol. Further purification by chromatography on silicic acid gel using chloroform as eluant.

Workup

  1. customThe product is produced
  2. customFurther purification by chromatography on silicic acid gel

Sources & evidence

ORD record
ord-a09c349d78a1485c896a642ef9f870a8
Source dataset
uspto-grants-1982_09
Patent number
US04349684

Reaction notes

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