Sodium Hydroxide → HCID 12961723, compound

HRID 1702906Notes

Reaction equation

HRID 1702906 reaction equation
C[O:2][C:3](=[O:35])[CH2:4][CH2:5][CH2:6][CH2:7][CH2:8][CH2:9][CH2:10][N:11]1[C:15]([C:16]2[CH:21]=[CH:20][CH:19]=[CH:18][CH:17]=2)=[C:14]([C:22]2[CH:27]=[CH:26][CH:25]=[CH:24][CH:23]=2)[N:13]([C:28]2[CH:33]=[CH:32][CH:31]=[CH:30][CH:29]=2)[C:12]1=[O:34].[OH-].[Na+]>CO>[O:34]=[C:12]1[N:13]([C:28]2[CH:29]=[CH:30][CH:31]=[CH:32][CH:33]=2)[C:14]([C:22]2[CH:27]=[CH:26][CH:25]=[CH:24][CH:23]=2)=[C:15]([C:16]2[CH:17]=[CH:18][CH:19]=[CH:20][CH:21]=2)[N:11]1[CH2:10][CH2:9][CH2:8][CH2:7][CH2:6][CH2:5][CH2:4][C:3]([OH:35])=[O:2]

Participants

4

Reactant 2

HCID 14798Sodium HydroxideHCID 54448380HCID 54448380, compound

Product 1

HCID 12961723HCID 12961723, compound

Reagents, catalysts & solvents 1

HCID 887MethanolSolvent

Procedure

The product is prepared as described in example 18 from 7.5 g of 8-(2-oxo-3.4.5-triphenyl-4-imidazolin-1-yl)-caprylic acid methyl ester and 0.64 g of NaOH in 30 cc. of methanol. Further purification by chromatography on silicic acid gel using chloroform as eluant.

Workup

  1. customThe product is prepared
  2. customFurther purification by chromatography on silicic acid gel

Sources & evidence

ORD record
ord-156c2b4b80ed4b1ab57118db2d66f8cb
Source dataset
uspto-grants-1982_09
Patent number
US04349684

Reaction notes

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