Sodium Hydroxide → HCID 12961725, compound

HRID 1702908Notes

Reaction equation

HRID 1702908 reaction equation
C[O:2][C:3](=[O:30])[CH2:4][CH2:5][CH2:6][CH2:7][CH2:8][CH2:9][CH2:10][N:11]1[C:15]([C:16]2[CH:21]=[CH:20][CH:19]=[CH:18][CH:17]=2)=[C:14]([C:22]2[CH:27]=[CH:26][CH:25]=[CH:24][CH:23]=2)[N:13]([CH3:28])[C:12]1=[O:29].[OH-].[Na+]>CO>[C:22]1([C:14]2[N:13]([CH3:28])[C:12](=[O:29])[N:11]([CH2:10][CH2:9][CH2:8][CH2:7][CH2:6][CH2:5][CH2:4][C:3]([OH:30])=[O:2])[C:15]=2[C:16]2[CH:21]=[CH:20][CH:19]=[CH:18][CH:17]=2)[CH:23]=[CH:24][CH:25]=[CH:26][CH:27]=1

Participants

4

Reactant 2

HCID 14798Sodium HydroxideHCID 54150617HCID 54150617, compound

Product 1

HCID 12961725HCID 12961725, compound

Reagents, catalysts & solvents 1

HCID 887MethanolSolvent

Procedure

The product is produced as described in example 18 from 17.5 g of 8-(4.5-diphenyl-3-methyl-2-oxo-4-imidazolin-1-yl) caprylic acid methyl ester and 2.1 g of NaOH in 100 cc. of methanol. Further purification by chromatography on silicic acid gel using chloroform as eluant.

Workup

  1. customThe product is produced
  2. customFurther purification by chromatography on silicic acid gel

Sources & evidence

ORD record
ord-aaf32a5174a74f039fca5e5c922803d9
Source dataset
uspto-grants-1982_09
Patent number
US04349684

Reaction notes

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