Participants
| Role | Name | HCID | Charge |
|---|
| Reactant | Benzene | HCID 241 | — |
| Reactant | Water | HCID 962 | — |
| Reactant | 16652-71-4 | HCID 3084256 | — |
| Solvent | Triethylamine | HCID 8471 | — |
| Product | Proline benzyl ester | HCID 99767 | 96.3% |
Reaction Steps
A mixture of 3.18 g of benzyl DL-prolinate hydrochloride, 3 ml of demineralized water, 25 ml of benzene and 1.34 g of triethylamine was stirred at 20° C. for one hour and the decanted organic phase was washed with water, dried and evaporated to dryness to obtain 2.6 g of benzyl DL-prolinate in the form of a colorless oil.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| Patent number | US04350637 |
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| Source dataset | uspto-grants-1982_09 |
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| ORD ID | ord-153135b6470e4fca92071a33cc510ba2 |
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| Source note | uspto-grants-1982_09 |
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