HuagongsheHuagongshe Chemistry Print Report · For research reference only
Perfluorooctanesulfonic acid → HCID 20553275, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Perfluorooctanesulfonic acid | HCID 74483 | — |
| Reactant | 1-(4-Isopropylphenyl)ethanamine | HCID 3728039 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | HCID 20553275 | HCID 20553275 | — |
Reaction Steps
The perfluoro-octylsulphonate salt was prepared by mixing a solution of 1-(4-isopropylphenyl)ethylamine (16.1 g) in ethanol (20 ml) with a solution of perfluoro-octylsulphonic acid (50 ml). The solution was evaporated to dryness and the residue was recrystallised from chloroform as soft colourless plates of 1-(4-isopropylphenyl) ethyl ammonium perfluoro-octyl sulphonate, melting point 158° C.(d). (Found: C 34.3; H 2.5; N 2.2%. C19H18F17NO3S requires: C 34.40; H 2.73; N 2.11%).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04350644 |
| Source dataset | uspto-grants-1982_09 |
| ORD ID | ord-6d585b59466345fe8cd212ca150b32da |
| Source note | uspto-grants-1982_09 |