HuagongsheHuagongshe Chemistry Print Report · For research reference only
Hydrochloric Acid → 3,4-Dimethyl-2-pentenoylchloride
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Hydrochloric Acid | HCID 313 | — |
| Reactant | Thionyl Chloride | HCID 24386 | — |
| Reactant | Ethyl 3,4-dimethyl-2-pentenoate | HCID 281491 | — |
| Solvent | Benzene | HCID 241 | — |
| Product | 3,4-Dimethyl-2-pentenoylchloride | HCID 54127392 | — |
Reaction Steps
3,4-Dimethyl-2-pentenoic acid (XI, 4.1 g) was heated to a gentle boil with thionyl chloride (50 g) in benzene (50 mL) until the generation of hydrochloric acid gas ceased. Removal of the excess thionyl chloride and benzene by evaporation in vacuo followed by a distillation of the reaction product gave pure 3,4-dimethyl-2-pentenoylchloride (IX, 64° C. (9.5 mm)).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04350638 |
| Source dataset | uspto-grants-1982_09 |
| ORD ID | ord-ca025f933d654ceab519a593a8a60d57 |
| Source note | uspto-grants-1982_09 |