HuagongsheHuagongshe Chemistry Print Report · For research reference only
Dimethyl Sulfate → 68256-20-2
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Dimethyl Sulfate | HCID 6497 | — |
| Reactant | Benzamide, 4-chloro-N-((1-ethyl-2-pyrrolidinyl)methyl)-2-methoxy-5-((methylsulfonyl)amino)- | HCID 3051978 | — |
| Product | 68256-20-2 | HCID 3051973 | — |
Reaction Steps
Using N-(1-ethyl-2-pyrrolidinylmethyl)-2-methoxy-4-chloro-5-methanesulfonamidobenzamide and dimethyl sulfate, the reaction is effected as in Example 5, whereby N-(1-ethyl-2-pyrrolidinylmethyl)-2-methoxy-4-chloro-5-(N-methylmethanesulfonamido)benzamide is obtained as crystals melting at 140.5° to 142° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04351770 |
| Source dataset | uspto-grants-1982_09 |
| ORD ID | ord-b26301bf1eea43a19324380eeb77e278 |
| Source note | uspto-grants-1982_09 |