HuagongsheHuagongshe Chemistry Print Report · For research reference only
Pyridinium chloride → HCID 12635628, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Pyridinium chloride | HCID 10176127 | — |
| Reactant | HCID 10331344 | HCID 10331344 | — |
| Product | HCID 12635628 | HCID 12635628 | — |
Reaction Steps
6-Methoxy-2,3-naphthalenedicarboxylic anhydride (4.0 g) and pyridine hydrochloride (8.0 g) were fused at 240° for 0.5 hr. in a nitrogen atmosphere. The flask contents were cooled, washed (water) and filtered to give a crude sample of 6-hydroxy-2,3-naphthalenedicarboxylic anhydride (m.p. 266°) which was used without purification.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04351842 |
| Source dataset | uspto-grants-1982_09 |
| ORD ID | ord-7f56794f7d1949d082d5103e11115454 |
| Source note | uspto-grants-1982_09 |