HuagongsheHuagongshe Chemistry Print Report · For research reference only
3,5-Dimethoxybenzoyl chloride → HCID 13064272, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 3,5-Dimethoxybenzoyl chloride | HCID 87003 | — |
| Reactant | methyl 1H-pyrrole-3-carboxylate | HCID 12361759 | — |
| Product | HCID 13064272 | HCID 13064272 | — |
Reaction Steps
By the procedure of Example 64, but a 5 hour reaction time, 3,5-dimethoxybenzoyl chloride (4.0 g., 20 mmoles) was reacted with methyl pyrrole-3-carboxylate to yield, without recrystallization, methyl 5-(3,5-dimethoxybenzoyl)pyrrole-3-carboxylate (3.7 g., m.p. 115°-120° C., m/e 289).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04351843 |
| Source dataset | uspto-grants-1982_09 |
| ORD ID | ord-0eb2e6ba47174ee9965bbd0212a93daa |
| Source note | uspto-grants-1982_09 |