Heptane → HCID 20400953, compound

HRID 1703316Notes

Reaction equation

HRID 1703316 reaction equation
[Cl:1][C:2]1[CH:16]=[CH:15][C:5]([O:6][C:7]2[CH:8]=[C:9]([C:12]([O-:14])=[O:13])[NH:10][CH:11]=2)=[CH:4][CH:3]=1.C([O-])(=O)CCCCCCC/C=C\CCCCCCCC.[Mg+2:37].C([O-])(=O)CCCCCCC/C=C\CCCCCCCC.CCCCCCC>C(O)C>[Cl:1][C:2]1[CH:16]=[CH:15][C:5]([O:6][C:7]2[CH:8]=[C:9]([C:12]([O-:14])=[O:13])[NH:10][CH:11]=2)=[CH:4][CH:3]=1.[Mg+2:37].[Cl:1][C:2]1[CH:16]=[CH:15][C:5]([O:6][C:7]2[CH:8]=[C:9]([C:12]([O-:14])=[O:13])[NH:10][CH:11]=2)=[CH:4][CH:3]=1

Participants

5

Reactant 3

HCID 8900HeptaneHCID 64332821555-53-9HCID 20401117HCID 20401117, compound

Product 1

HCID 20400953HCID 20400953, compound

Reagents, catalysts & solvents 1

HCID 702EthanolSolvent

Procedure

4-(4-Chlorophenoxy)pyrrole-2-carboxylate and an equivalent quantity of magnesium oleate are each dissolved in ethanol and the solutions mixed. Magnesium 4-(4-chlorophenoxy)pyrrole-2-carboxylate is isolated by concentration and/or addition of heptane.

Workup

  1. additionthe solutions mixed

Sources & evidence

ORD record
ord-ec0291238d584081b33b70d66fc85dd9
Source dataset
uspto-grants-1982_09
Patent number
US04351843

Reaction notes

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