HuagongsheHuagongshe Chemistry Print Report · For research reference only
Formic Acid → N-Pyridin-2-ylmethyl-formamide
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Formic Acid | HCID 284 | — |
| Reactant | 2-Pyridinemethanamine | HCID 19509 | — |
| Product | N-Pyridin-2-ylmethyl-formamide | HCID 12228441 | — |
Reaction Steps
2-Aminomethylpyridine (60 g.) was refluxed with 180 ml. of formic acid for 4 hours and left to stir for approximately 16 hours at room temperature. The reaction mixture was concentrated to an oil and purified; 2-formamidomethylpyridine obtained by distillation (72.3 g., b.p. 117°-141° C./0.5 mm.)
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04351843 |
| Source dataset | uspto-grants-1982_09 |
| ORD ID | ord-519f8ef8a22241f9b224efb801894970 |
| Source note | uspto-grants-1982_09 |