HuagongsheHuagongshe Chemistry Print Report · For research reference only
Triphenylarsine → 2,6-Dichlorophenol
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Triphenylarsine | HCID 11773 | — |
| Reactant | 2,2,6,6-Tetrachlorocyclohexan-1-one | HCID 77407 | — |
| Product | 2,6-Dichlorophenol | HCID 6899 | 79.3% |
Reaction Steps
190 g (0.8 mol) of 2,2,6,6-tetrachlorocyclohexanone and 3 g (0.065 mol) of triphenylarsine were introduced into the reactor used in Example 1. The reaction mixture was heated at 150°-180° C., under stirring. Same was then treated as in Example 1 to yield 103.4 g of 2,6-dichlorophenol.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04351969 |
| Source dataset | uspto-grants-1982_09 |
| ORD ID | ord-322dcdc1ee6442148bc1f280d8ee52cb |
| Source note | uspto-grants-1982_09 |