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HRID1703397

反应详情

EQUATION

反应方程式

HRID 1703397 的结构方程式

REACTANTS

反应物

2
结构：O=S(=O)(Cl)Cl
HCID24648

Sulfuryl chloride

Cl2O2S

结构：COC(=O)c1ccc(OC)cc1N
HCID12919999

Methyl 2-amino-4-methoxybenzoate

C9H11NO3

PRODUCTS

生成物

1
结构：COC(=O)c1cc(Cl)c(OC)cc1N
HCID12920001

Benzoic acid, 2-amino-5-chloro-4-methoxy-, methyl ester

C9H10ClNO3

收率 90%

PROCEDURE

实验过程

Treatment of methyl-4-methoxyanthranilate with sulfuryl chloride as described above afforded methyl-4-methoxy-5-chloroanthranilate, M.P., 197°-200° C. in 90% yield.