HuagongsheHuagongshe Chemistry Print Report · For research reference only
Tetrahydrofuran → HCID 22761655, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Tetrahydrofuran | HCID 8028 | — |
| Reactant | HCID 22761648 | HCID 22761648 | — |
| Catalyst | HCID 178418647 | HCID 178418647 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | HCID 22761655 | HCID 22761655 | — |
Reaction Steps
The starting material is prepared as follows: The solution of 2 g of N-(4-nitro-2-iodomethylphenyl)-4-chlorophthalimide in 25 ml of tetrahydrofuran and 25 ml of ethanol, is stirred with 8.7 g of freshly prepared silver carbonate for 20 hours, with protection from light. The mixture is filtered and the filtrate evaporated, to yield the N-(2-ethoxymethyl-4-nitrophenyl)-4-chlorophthalimide.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04124593 |
| Source dataset | uspto-grants-1978_11 |
| ORD ID | ord-a5aedfb9d4c84437a80d9b95961e57df |
| Source note | uspto-grants-1978_11 |