Acetic Acid → HCID 22761653, compound

Participants

Reaction Steps

The starting material is prepared as follows: The solution of 1.77 g of N-(4-nitro-2-iodomethylphenyl)-4-chlorophthalimide and 1.0 g of silver acetate in 32 ml of acetic acid is refluxed for one hour with protection from light. It is filtered, the filtrate evaporated and the residue recrystallized from ethyl acetate-diethyl ether, to yield the N-(2-acetoxymethyl-4-nitrophenyl)-4-chlorophthalimide melting at 124°-125°.

Provenance & Evidence