HuagongsheHuagongshe Chemistry Print Report · For research reference only
Sodium amide → HCID 54119240, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Sodium amide | HCID 24533 | — |
| Reactant | 4-(2-Chloroethyl)morpholine | HCID 76727 | — |
| Reactant | Phenyl(tricyclo[2.2.1.0~2,6~]heptan-3-yl)methanone | HCID 94017 | — |
| Solvent | Toluene | HCID 1140 | — |
| Product | HCID 54119240 | HCID 54119240 | — |
Reaction Steps
A solution of 19.83 g. (0.1 mol) of tricyclo-(2.2.1.02.6)hept-3-yl phenyl ketone in 45 ml. of anhydrous toluene was added while stirring and boiling to a suspension of 3.9 g. (0.1 mol) of sodium amide in 45 ml. of anhydrous toluene, followed by etherification with a solution of 14.96 g. (0.1 mol) of N-(2-chloroethyl)-morpholine in 45 ml. of anhydrous toluene in the same way as in Example 3.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04124716 |
| Source dataset | uspto-grants-1978_11 |
| ORD ID | ord-1f0a4fb9e57246888d7d0d85a40d0038 |
| Source note | uspto-grants-1978_11 |