HuagongsheHuagongshe Chemistry Print Report · For research reference only
1-Cyano-2-ethoxy-2-methylaminoethylene → HCID 178483853, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 1-Cyano-2-ethoxy-2-methylaminoethylene | HCID 73683202 | — |
| Reactant | HCID 178433288 | HCID 178433288 | — |
| Solvent | Pyridine | HCID 1049 | — |
| Product | HCID 178483853 | HCID 178483853 | — |
Reaction Steps
4-Methyl-5-[(2-aminoethyl)thiomethyl]imidazole (3.5 g) was added to a solution of 1-cyano-2-ethoxy-2-methylaminoethylene in pyridine (3.1 g) and the solution was stirred for 5 hours at 100°. The product was chromatographed on a column of neutral alumina with elution by chloroform/ethyl acetate (1:1) to give the title compound as a glass.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04124717 |
| Source dataset | uspto-grants-1978_11 |
| ORD ID | ord-e897978022aa45c7a4b1d605e55179f7 |
| Source note | uspto-grants-1978_11 |