3,3-Dimethoxyprop-2-enenitrile → HCID 178495317, Verbindung
Reaktionsgleichung
[C:1]([CH:3]=[C:4](OC)[O:5][CH3:6])#[N:2].[CH3:9][C:10]1[N:11]=[CH:12][NH:13][C:14]=1[CH2:15][S:16][CH2:17][CH2:18][NH2:19]>>[C:1]([CH:3]=[C:4]([O:5][CH3:6])[NH:19][CH2:18][CH2:17][S:16][CH2:15][C:14]1[NH:13][CH:12]=[N:11][C:10]=1[CH3:9])#[N:2]Komponenten
3
Versuchsvorschrift
Reaction of 1-cyano-2,2-bis methoxyethylene (J.A.C.S., 1949, 71, 47) with 4-methyl-5-[(2-aminoethyl)thiomethyl]imidazole by the procedure of Example 8(i) yields 1-cyano-2-methoxy-2-[2-((4-methyl-5-imidazolyl)methylthio)ethylamino]ethylene. (ii) Reaction of this methylthio compound with 2-(3-aminopropylthio)oxazole by the procedure of Example 1(a) (ii) gives the title compound.
Quellen und Nachweise
- ORD-Eintrag
- ord-432aac77f9c0433793d72063010bbe12
- Quelldatensatz
- uspto-grants-1978_11
- Patentnummer
- US04124717
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