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HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
HRID 1703637Erstellt: 25. Oktober 2026

Ammonia → HCID 178494684, Verbindung

https://huagongshe.com/reaction/1703637

Reaktionsgleichung

Beteiligte Stoffe

RolleNameHCIDEinwaage
EduktAmmoniaHCID 222—
EduktDihydroxyacetoneHCID 670—
EduktEthyl 2-methoxyethanecarboximidate hydrochlorideHCID 12816254—
ProduktHCID 178494684HCID 178494684—

Reaktionsschritte

A 307.2 gm. portion of ethyl 2-methoxyacetimidate hydrochloride [Rule, J. Chem. Soc. 113, 9 (1918)] and 180 gm. of 1,3-dihydroxyacetone in one liter of liquid ammonia are reacted as described in Example 3 giving the desired product as an oil. A crystalline picrate salt (m.p. 175°-178° C.) is obtained by heating the oily product and picric acid in water.

Herkunft & Nachweise

DOI10.6084/m9.figshare.5104873.v1
PatentnummerUS04124766
Quelldatensatzuspto-grants-1978_11
ORD IDord-1a7290f08cdb4f098ba2c625539dd8c0
Quellennotizuspto-grants-1978_11