HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
Ammonia → HCID 178494684, Verbindung
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|---|---|---|
| Edukt | Ammonia | HCID 222 | — |
| Edukt | Dihydroxyacetone | HCID 670 | — |
| Edukt | Ethyl 2-methoxyethanecarboximidate hydrochloride | HCID 12816254 | — |
| Produkt | HCID 178494684 | HCID 178494684 | — |
Reaktionsschritte
A 307.2 gm. portion of ethyl 2-methoxyacetimidate hydrochloride [Rule, J. Chem. Soc. 113, 9 (1918)] and 180 gm. of 1,3-dihydroxyacetone in one liter of liquid ammonia are reacted as described in Example 3 giving the desired product as an oil. A crystalline picrate salt (m.p. 175°-178° C.) is obtained by heating the oily product and picric acid in water.
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patentnummer | US04124766 |
| Quelldatensatz | uspto-grants-1978_11 |
| ORD ID | ord-1a7290f08cdb4f098ba2c625539dd8c0 |
| Quellennotiz | uspto-grants-1978_11 |