HuagongsheHuagongshe Chemistry Print Report · For research reference only
2-Bromobenzoic acid → 2-Bromo-5-(chlorosulfonyl)benzoic acid
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2-Bromobenzoic acid | HCID 6940 | — |
| Reactant | 2-Methylpiperidine | HCID 7974 | — |
| Reactant | Chlorosulfonic acid | HCID 24638 | — |
| Product | 2-Bromo-5-(chlorosulfonyl)benzoic acid | HCID 3427298 | — |
Reaction Steps
2-Bromo-5-chlorosulfonylbenzoic acid is prepared by reacting o-bromobenzoic acid with chlorosulfonic acid by the method of Example 1. This is reacted with 2-methylpiperidine by the procedure of Example 6. Recrystallization from acetone-hexane yields the product, m.p. 148°-150° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04124590 |
| Source dataset | uspto-grants-1978_11 |
| ORD ID | ord-1b96727bac174285a33ba814069f239c |
| Source note | uspto-grants-1978_11 |