Toluene → HCID 22759797, compound

HRID 1703749Notes

Reaction equation

HRID 1703749 reaction equation
CC(O)(C[NH2:5])C.[CH2:7]([CH:16]1[CH2:21][CH2:20][C:19](=[O:22])[CH2:18][CH2:17]1)[CH2:8][CH2:9][CH2:10][CH2:11][CH2:12][CH2:13][CH2:14][CH3:15].[C:23]1([CH3:29])[CH:28]=CC=C[CH:24]=1>>[CH3:24][C:23]1([CH3:29])[NH:5][C:19]2([CH2:18][CH2:17][CH:16]([CH2:7][CH2:8][CH2:9][CH2:10][CH2:11][CH2:12][CH2:13][CH2:14][CH3:15])[CH2:21][CH2:20]2)[O:22][CH2:28]1

Participants

4

Reactant 3

HCID 1140TolueneHCID 951022-Propanol, 1-amino-2-methyl-HCID 11075070HCID 11075070, compound

Product 1

HCID 22759797HCID 22759797, compound

Procedure

The procedure of Example 1 was followed utilizing 1,1-dimethylethanolamine (2.7 grams; 0.03 mole) and 4-n-nonylcyclohexanone (6.73 grams; 0.03 mole) in 100 mls of toluene. After removing the toluene, the residue was distilled to obtain 4.3 grams (48.5% of theoretical; b.p. 113°-115° C. at 0.01 mm.) of the desired product.

Workup

  1. customAfter removing the toluene
  2. distillationthe residue was distilled

Sources & evidence

ORD record
ord-2512a5b88f604df7a9a333b22a07f1fb
Source dataset
uspto-grants-1978_11
Patent number
US04125518

Reaction notes

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