Toluene → HCID 10900788, compound

HRID 1703750Notes

Reaction equation

HRID 1703750 reaction equation
CC(O)(C[NH2:5])C.[CH3:7][C:8]([CH2:10][CH2:11][CH2:12][CH2:13][CH2:14][CH2:15][CH2:16][CH2:17][CH3:18])=[O:9].[C:19]1([CH3:25])[CH:24]=CC=C[CH:20]=1>>[CH2:10]([C:8]1([CH3:7])[NH:5][C:19]([CH3:25])([CH3:24])[CH2:20][O:9]1)[CH2:11][CH2:12][CH2:13][CH2:14][CH2:15][CH2:16][CH2:17][CH3:18]

Participants

4

Reactant 3

HCID 1140TolueneHCID 81632-UndecanoneHCID 951022-Propanol, 1-amino-2-methyl-

Product 1

HCID 10900788HCID 10900788, compound

Procedure

The procedure of Example 1 was followed utilizing 1,1-dimethylethanolamine (22.3 grams; 0.25 mole) and methyl n-nonylketone (42.6 grams; 0.25 mole) in 250 mls of toluene. After removing the toluene, the residue was distilled to obtain 26.7 grams (44% of theoretical; b.p. 92°-94° C. at 0.3 mm.) of the desired product. This product was prepared for comparison with the compounds of Examples 1-3.

Workup

  1. customAfter removing the toluene
  2. distillationthe residue was distilled

Sources & evidence

ORD record
ord-21ee2a3c50d447a8878c7457c9723fbd
Source dataset
uspto-grants-1978_11
Patent number
US04125518

Reaction notes

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