HuagongsheHuagongshe Chemistry Print Report · For research reference only
Hydrogen Bromide → HCID 86736145, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Hydrogen Bromide | HCID 260 | — |
| Reactant | 3-(4-Iodophenyl)butan-1-ol | HCID 43206 | — |
| Reactant | Thiourea | HCID 2723790 | — |
| Solvent | Water | HCID 962 | — |
| Product | HCID 86736145 | HCID 86736145 | 41% |
Reaction Steps
70 g of 3-(p-iodophenyl) butanol was combined in solution with 138 g of hydrobromic acid (48%) and 20 g thiourea in 100 ml of water and the thiol product vacuum distilled at 126° and 0.18 mm Hg. A 41% yield of 3-(p-Iodophenyl) butane thiol was confirmed having a refractive index of n25D = 1.6071 and nmr, ir and gc readings commensurate with the structure of the desired product.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04125554 |
| Source dataset | uspto-grants-1978_11 |
| ORD ID | ord-a570eb0d6d32463ab7ca54be87b9cf08 |
| Source note | uspto-grants-1978_11 |