HuagongsheHuagongshe Chemistry Print Report · For research reference only
Hydrogen Bromide → 3-(p-Iodophenyl) propane thiol
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Hydrogen Bromide | HCID 260 | — |
| Reactant | Thiourea | HCID 2723790 | — |
| Reactant | 4-Iodobenzenepropanol | HCID 3042614 | — |
| Solvent | Water | HCID 962 | — |
| Product | 3-(p-Iodophenyl) propane thiol | HCID 86736146 | 66% |
Reaction Steps
62 g of 3-(p-iodophenyl) propanol was combined in solution with 161 g of hydrobromic acid (48%) and 23 g of thiourea in 100 ml of water and the thiol product vacuum distilled at 114°-117° and 0.1 mm Hg. A 66% yield of 3-(p-iodophenyl) propane thiol was confirmed having a refractive index of n25D = 1.6202.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04125554 |
| Source dataset | uspto-grants-1978_11 |
| ORD ID | ord-709e455cfe3c4e67b2a9fa9cea4fd45c |
| Source note | uspto-grants-1978_11 |