HuagongsheHuagongshe Chemistry Print Report · For research reference only
Diisopropylamine → HCID 22760800, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Diisopropylamine | HCID 7912 | — |
| Reactant | Citraconic Anhydrides | HCID 12012 | — |
| Reactant | 2-Methyl-1-sulfanylheptan-2-OL | HCID 13506860 | — |
| Product | HCID 22760800 | HCID 22760800 | — |
Reaction Steps
Analogously to Example 1, from citraconic acid anhydride and 2-hydroxy-2-methylheptane-1-thiol in the presence of diisopropylamine and the usual working up of the reaction mixture, 3,6-dimethyl-2-oxo-6-pentyl-1,4-oxathiane-3-acetic acid is obtained. Using chromatographic purification it can be separated into two isomers:
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04125622 |
| Source dataset | uspto-grants-1978_11 |
| ORD ID | ord-88a614bddf9f4825b895341ace199a07 |
| Source note | uspto-grants-1978_11 |