Participants
| Role | Name | HCID | Charge |
|---|
| Reactant | Ammonia | HCID 222 | — |
| Reactant | Methanol | HCID 887 | — |
| Reactant | HCID 12557652 | HCID 12557652 | — |
| Product | HCID 12557669 | HCID 12557669 | — |
Reaction Steps
A solution of 2,4-dimethoxy-2,4,6-cycloheptatrien-1-one [described above in (b), 2.4 g] in methanol (70) is cooled to -25° C and saturated with ammonia gas. The solution is heated in a pressure bottle at 80° C for 4 hours and cooled to -70° C. The pressure bottle is opened and the solvent is evaporated to give 2-amino-4-methoxy-2,4,6-cycloheptatrien-1-one.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| Patent number | US04125625 |
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| Source dataset | uspto-grants-1978_11 |
|---|
| ORD ID | ord-edd98953765a4982af53c0144a991832 |
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| Source note | uspto-grants-1978_11 |
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