HuagongsheHuagongshe Chemistry Print Report · For research reference only
Diethyl Ether → HCID 22760541, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Diethyl Ether | HCID 3283 | — |
| Reactant | N,N'-Di-sec-butylthiourea | HCID 5366322 | — |
| Reactant | 2,4'-Dichloro-3'-sulfamoylacetophenone | HCID 21316749 | — |
| Solvent | Ethyl Acetate | HCID 8857 | — |
| Product | HCID 22760541 | HCID 22760541 | — |
Reaction Steps
5.3 g of 2,4'-dichloro-3'-sulfamoylacetophenone and 3.8 g of 1,3-di-sec.-butylthiourea was reacted in the manner described in Example 16, the reaction mixture was introduced into a solution of 40 ml of diethyl ether and 120 ml of ethyl acetate and the colorless, crystalline end product was filtered off after stirring for 4 hours at room temperature. Melting point: 186° C. (decomposition).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04125614 |
| Source dataset | uspto-grants-1978_11 |
| ORD ID | ord-5f041466681f43f39620bb072f3d432a |
| Source note | uspto-grants-1978_11 |