N,N'-Bis(2-methylpropyl)thiourea → HCID 22760584, compound

HRID 1703852Notes

Reaction equation

HRID 1703852 reaction equation
[Cl:1][CH2:2][C:3]([C:5]1[CH:10]=[CH:9][C:8]([Cl:11])=[C:7]([S:12](=[O:15])(=[O:14])[NH2:13])[CH:6]=1)=[O:4].[CH2:16]([NH:20][C:21]([NH:23][CH2:24][CH:25]([CH3:27])[CH3:26])=[S:22])[CH:17]([CH3:19])[CH3:18]>>[ClH:1].[Cl:11][C:8]1[CH:9]=[CH:10][C:5]([C:3]2([OH:4])[CH2:2][S:22][C:21](=[N:20][CH2:16][CH:17]([CH3:18])[CH3:19])[N:23]2[CH2:24][CH:25]([CH3:27])[CH3:26])=[CH:6][C:7]=1[S:12](=[O:15])(=[O:14])[NH2:13]

Participants

3

Reactant 2

HCID 3035343N,N'-Bis(2-methylpropyl)thioureaHCID 213167492,4'-Dichloro-3'-sulfamoylacetophenone

Product 1

HCID 22760584HCID 22760584, compound

Procedure

5.3 g of 2,4'-dichloro-3'-sulfamoylacetophenone and 3.8 g of 1,3-diisobutylthiourea were reacted according to the prescription made in Example 16 and worked up as described in Example 25. Colorless, crystalline end product: melting point: 176° C. (decomposition).

Sources & evidence

ORD record
ord-1dd86767222740088b7e0675901b1063
Source dataset
uspto-grants-1978_11
Patent number
US04125614

Reaction notes

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