4-(4-Chloro-3-sulfamoylphenyl)-2-isobutylimino-3-methyl-1,3-thiazolidine-4-ol-hydrobromide → 4-(4-Chloro-3-sulfamoylphenyl)-2-isobutylimino-3-methyl-1,3-thiazolidine-4-ol

HRID 1703854Notes

Reaction equation

HRID 1703854 reaction equation
Br.[Cl:2][C:3]1[CH:8]=[CH:7][C:6]([C:9]2([OH:20])[CH2:13][S:12][C:11](=[N:14][CH2:15][CH:16]([CH3:18])[CH3:17])[N:10]2[CH3:19])=[CH:5][C:4]=1[S:21](=[O:24])(=[O:23])[NH2:22]>O>[Cl:2][C:3]1[CH:8]=[CH:7][C:6]([C:9]2([OH:20])[CH2:13][S:12][C:11](=[N:14][CH2:15][CH:16]([CH3:17])[CH3:18])[N:10]2[CH3:19])=[CH:5][C:4]=1[S:21](=[O:23])(=[O:24])[NH2:22]

Participants

3

Reactant 1

HCID 227604724-(4-Chloro-3-sulfamoylphenyl)-2-isobutylimino-3-methyl-1,3-thiazolidine-4-ol-hydrobromide

Product 1

HCID 227604734-(4-Chloro-3-sulfamoylphenyl)-2-isobutylimino-3-methyl-1,3-thiazolidine-4-ol

Reagents, catalysts & solvents 1

HCID 962WaterSolvent

Procedure

8 g of 4-(4-chloro-3-sulfamoylphenyl)-2-isobutylimino-3-methyl-1,3-thiazolidine-4-ol-hydrobromide were dissolved in 30 ml of water and the end product was precipitated by pouring it into 20 ml of a saturated and stirred sodium carbonate solution. Colorless, amorphous solid body, γC=N 1615 cm-1.

Workup

  1. customthe end product was precipitated
  2. additionby pouring it into 20 ml of a saturated and

Sources & evidence

ORD record
ord-b640613de76e4e8dbbfc673d9c590f2e
Source dataset
uspto-grants-1978_11
Patent number
US04125614

Reaction notes

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