HuagongsheHuagongshe Chemistry Print Report · For research reference only
1,3-(Dihexyl)thiourea → 4-(4-Chloro-3-sulfamoylphenyl)-3-n-hexyl-2-n-hexylimino-1,3-thiazolidine-4-ol-hydrochloride
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 1,3-(Dihexyl)thiourea | HCID 2801208 | — |
| Reactant | 2,4'-Dichloro-3'-sulfamoylacetophenone | HCID 21316749 | — |
| Product | 4-(4-Chloro-3-sulfamoylphenyl)-3-n-hexyl-2-n-hexylimino-1,3-thiazolidine-4-ol-hydrochloride | HCID 22760537 | — |
Reaction Steps
5.2 g of 2,4'-dichloro-3'-sulfamoylacetophenone and 4.8 g of 1,3-di-n-hexyl-thiourea were reacted according to the prescription given in Example 12, the end product was precipitated with diethyl ether and the remaining oil was treated with cyclohexane. Colorless, amorphous solid body: decomposition beginning at 75° C., γ C=N 1615 cm-1.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04125614 |
| Source dataset | uspto-grants-1978_11 |
| ORD ID | ord-6e81d5a1aa064cc7b2946063bac49d3f |
| Source note | uspto-grants-1978_11 |