Bromo-4'-chloro-3'-sulfamoylacetophenone → HCID 22760469, compound

HRID 1703858Notes

Reaction equation

HRID 1703858 reaction equation
[Br:1][CH2:2][C:3]([C:5]1[CH:10]=[CH:9][C:8]([Cl:11])=[C:7]([S:12](=[O:15])(=[O:14])[NH2:13])[CH:6]=1)=[O:4].[CH2:16]([NH:19][C:20]([NH:22][CH:23]1[CH2:25][CH2:24]1)=[S:21])[CH:17]=[CH2:18]>>[BrH:1].[CH2:16]([N:19]1[C:3]([C:5]2[CH:10]=[CH:9][C:8]([Cl:11])=[C:7]([S:12](=[O:15])(=[O:14])[NH2:13])[CH:6]=2)([OH:4])[CH2:2][S:21][C:20]1=[N:22][CH:23]1[CH2:25][CH2:24]1)[CH:17]=[CH2:18]

Participants

3

Reactant 2

HCID 12952390Bromo-4'-chloro-3'-sulfamoylacetophenoneHCID 17379841HCID 17379841, compound

Product 1

HCID 22760469HCID 22760469, compound

Procedure

6.2 g of 2-bromo-4'-chloro-3'-sulfamoylacetophenone and 3.1 g of 1-allyl-3-cyclopropylthiourea were reacted and worked up according to the prescription given in Example 12. Colorless, amorphous solid body: decomposition beginning at 90° C., γC=N 1600 cm-1.

Workup

  1. custombeginning at 90° C.

Sources & evidence

ORD record
ord-1f9d43386ad040b6852753e64b47905e
Source dataset
uspto-grants-1978_11
Patent number
US04125614

Reaction notes

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