HuagongsheHuagongshe Chemistry Print Report · For research reference only
Dicyclohexylthiourea → 4-(4-Chloro-3-sulfamoylphenyl)-3-cyclohexyl-2-cyclohexylimino-1,3-thiazolidine-4-ol-hydrochloride
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Dicyclohexylthiourea | HCID 727200 | — |
| Reactant | 2,4'-Dichloro-3'-sulfamoylacetophenone | HCID 21316749 | — |
| Product | 4-(4-Chloro-3-sulfamoylphenyl)-3-cyclohexyl-2-cyclohexylimino-1,3-thiazolidine-4-ol-hydrochloride | HCID 22760523 | — |
Reaction Steps
5.2 g of 2,4'-dichloro-3'-sulfamoylacetophenone and 4.8 g of 1,3-dicyclohexylthiourea were reacted according to the prescription made in Example 12, the end product was precipitated with 200 ml of diethyl ether and the oil was crystallized after decanting the solvent with diethyl ether. Colorless, crystalline solid body: melting point: 177° C. (from acrylonitrile).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04125614 |
| Source dataset | uspto-grants-1978_11 |
| ORD ID | ord-a543b54f56c94c3ea051611ffba51ac8 |
| Source note | uspto-grants-1978_11 |