HCID 2808837, compound → 59814-99-2

HRID 1703872Notes

Reaction equation

HRID 1703872 reaction equation
[Br:1][CH2:2][C:3]([C:5]1[CH:10]=[CH:9][C:8]([Cl:11])=[C:7]([S:12](=[O:15])(=[O:14])[NH2:13])[CH:6]=1)=[O:4].[O:16]1[CH:20]=[CH:19][CH:18]=[C:17]1[CH2:21][NH:22][C:23]([NH:25][CH3:26])=[S:24]>>[BrH:1].[Cl:11][C:8]1[CH:9]=[CH:10][C:5]([C:3]2([OH:4])[CH2:2][S:24][C:23](=[N:22][CH2:21][C:17]3[O:16][CH:20]=[CH:19][CH:18]=3)[N:25]2[CH3:26])=[CH:6][C:7]=1[S:12](=[O:15])(=[O:14])[NH2:13]

Participants

3

Reactant 2

HCID 2808837HCID 2808837, compoundHCID 12952390Bromo-4'-chloro-3'-sulfamoylacetophenone

Product 1

HCID 2276057359814-99-2

Procedure

4.7 g of 2-bromo-4'-chloro-3'-sulfamoylacetophenone and 2.55 g of 1-(2-furylmethyl)-3-methylthiourea were reacted according to the prescription of Example 23 and the end product was precipitated by adding 100 ml of diethyl ether. Colorless crystalline solid body: melting point: 168° C. (decomposition).

Workup

  1. customthe end product was precipitated
  2. additionby adding 100 ml of diethyl ether

Sources & evidence

ORD record
ord-83062ac79e2048ad86a17b9755578219
Source dataset
uspto-grants-1978_11
Patent number
US04125614

Reaction notes

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