Bromo-4'-chloro-3'-sulfamoylacetophenone → HCID 22760583, compound

HRID 1703873Notes

Reaction equation

HRID 1703873 reaction equation
[Br:1][CH2:2][C:3]([C:5]1[CH:10]=[CH:9][C:8]([Cl:11])=[C:7]([S:12](=[O:15])(=[O:14])[NH2:13])[CH:6]=1)=[O:4].[CH3:16][NH:17][C:18]([NH:20][CH2:21][CH:22]([O:24][CH3:25])[CH3:23])=[S:19]>>[BrH:1].[Cl:11][C:8]1[CH:9]=[CH:10][C:5]([C:3]2([OH:4])[CH2:2][S:19][C:18](=[N:20][CH2:21][CH:22]([O:24][CH3:25])[CH3:23])[N:17]2[CH3:16])=[CH:6][C:7]=1[S:12](=[O:15])(=[O:14])[NH2:13]

Participants

3

Reactant 2

HCID 12952390Bromo-4'-chloro-3'-sulfamoylacetophenoneHCID 22760462HCID 22760462, compound

Product 1

HCID 22760583HCID 22760583, compound

Procedure

4.7 g of 2-bromo-4'-chloro-3'-sulfamoylacetophenone and 2.19 g of 1-methyl-3-(2-methoxypropyl)-thiourea were reacted as prescribed in Example 23 and the crystalline end product was filtered off. Colorless solid crystals: melting point: 167° C. (decomposition).

Workup

  1. filtrationthe crystalline end product was filtered off

Sources & evidence

ORD record
ord-e5d3477dcfd24be5927527b91d1d1ccf
Source dataset
uspto-grants-1978_11
Patent number
US04125614

Reaction notes

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